Temperature standard reference materials for thermal analysis
Identifieur interne : 000297 ( Main/Exploration ); précédent : 000296; suivant : 000298Temperature standard reference materials for thermal analysis
Auteurs : RBID : ISTEX:10973_1992_Article_BF01979632.pdfEnglish descriptors
Abstract
The feasibility of the use of potassium nitrate and potassium perchlorate as temperature standards in Differential scanning calorimetry has been studied. The solid-state phase transition temperatures of KNO3 and KClO4 were determined by means of DSC. The metrological properties of these salts as calibration materials were examined. The reliability of KNO3 and KClO4 calibrations was investigated by twofold determination of the bismuth melting temperature after the apparatus had been calibrated with indium and lead, and with KNO3 and KClO4. Conclusions were drawn concerning the suitability of these salts for use as DSC temperature calibrants.
DOI: 10.1007/BF01979632
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<record><TEI><teiHeader><fileDesc><titleStmt><title>Temperature standard reference materials for thermal analysis</title><author><name>K. Kostyrko</name><affiliation wicri:level="1"><mods:affiliation>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw, Poland</mods:affiliation><country xml:lang="fr">Pologne</country><wicri:regionArea>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw</wicri:regionArea><wicri:noRegion>Warsaw</wicri:noRegion></affiliation></author><author><name>M. Skoczylas</name><affiliation wicri:level="1"><mods:affiliation>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw, Poland</mods:affiliation><country xml:lang="fr">Pologne</country><wicri:regionArea>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw</wicri:regionArea><wicri:noRegion>Warsaw</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="RBID">ISTEX:10973_1992_Article_BF01979632.pdf</idno><date when="1992">1992</date><idno type="doi">10.1007/BF01979632</idno><idno type="wicri:Area/Main/Corpus">000886</idno><idno type="wicri:Area/Main/Curation">000886</idno><idno type="wicri:Area/Main/Exploration">000297</idno></publicationStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>DSC temperature calibrants</term><term>Potassium nitrate</term><term>Potassium perchlorate</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="eng">The feasibility of the use of potassium nitrate and potassium perchlorate as temperature standards in Differential scanning calorimetry has been studied. The solid-state phase transition temperatures of KNO3 and KClO4 were determined by means of DSC. The metrological properties of these salts as calibration materials were examined. The reliability of KNO3 and KClO4 calibrations was investigated by twofold determination of the bismuth melting temperature after the apparatus had been calibrated with indium and lead, and with KNO3 and KClO4. Conclusions were drawn concerning the suitability of these salts for use as DSC temperature calibrants.</div></front></TEI><mods xsi:schemaLocation="http://www.loc.gov/mods/v3 file:///applis/istex/home/loadistex/home/etc/xsd/mods.xsd" version="3.4" istexId="9ac17444c3fc0148391af166c38984e5f4802268"><titleInfo lang="eng"><title>Temperature standard reference materials for thermal analysis</title></titleInfo><name type="personal"><namePart type="given">K.</namePart><namePart type="family">Kostyrko</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw, Poland</affiliation></name><name type="personal"><namePart type="given">M.</namePart><namePart type="family">Skoczylas</namePart><role><roleTerm type="text">author</roleTerm></role><affiliation>Polish Committee for Standardization, Measures and Quality Control, Elektoralna 2, 00-139, Warsaw, Poland</affiliation></name><typeOfResource>text</typeOfResource><genre>Original Paper</genre><originInfo><publisher>Kluwer Academic Publishers, Dordrecht</publisher><dateValid encoding="w3cdtf">2005-07-07</dateValid><copyrightDate encoding="w3cdtf">1992</copyrightDate></originInfo><language><languageTerm type="code" authority="iso639-2b">eng</languageTerm></language><physicalDescription><internetMediaType>text/html</internetMediaType></physicalDescription><abstract lang="eng">The feasibility of the use of potassium nitrate and potassium perchlorate as temperature standards in Differential scanning calorimetry has been studied. The solid-state phase transition temperatures of KNO3 and KClO4 were determined by means of DSC. The metrological properties of these salts as calibration materials were examined. The reliability of KNO3 and KClO4 calibrations was investigated by twofold determination of the bismuth melting temperature after the apparatus had been calibrated with indium and lead, and with KNO3 and KClO4. Conclusions were drawn concerning the suitability of these salts for use as DSC temperature calibrants.</abstract><abstract lang="ger">Es wurde die Möglichkeit der Verwendung von Kaliumnitrat und Kaliumperchlorat als Temperaturstandard für DSC untersucht. Die Bestimmung der Temperaturen für Feststoff-Phasenumwandlungen von Kaliumnitrat und Kaliumperchlorat wurde mittels DSC erreicht. Weiterhin wurden die meßtechnischen Eigenschaften der untersuchten Salze (KNO3 und KClO4) als Bezugssubstanzen geprüft. Die Zuverlässigkeit der Kalibrierung mittels KNO3 und KClO4 wurde durch eine zweifache Bestimmung der Schmelztemperatur von Wismut überprüft: einmal nach der Kalibrierung des Gerätes mit Indium und Blei und andererseits nach der Kalibrierung mit Kaliumnitrat und Kaliumperchlorat. Angesichts der Resultate kann man feststellen, daß die untersuchten Salze zur Temperaturkalibrierung in der DSC geeignet sind.</abstract><subject lang="eng"><genre>Keywords</genre><topic>DSC temperature calibrants</topic><topic>potassium nitrate</topic><topic>potassium perchlorate</topic></subject><relatedItem type="series"><titleInfo type="abbreviated"><title>Journal of Thermal Analysis</title></titleInfo><titleInfo><title>Journal of thermal analysis</title><partNumber>Year: 1992</partNumber><partNumber>Volume: 38</partNumber><partNumber>Number: 9</partNumber></titleInfo><genre>Archive Journal</genre><originInfo><dateIssued encoding="w3cdtf">1992-09-01</dateIssued><copyrightDate encoding="w3cdtf">1992</copyrightDate></originInfo><subject usage="primary"><topic>Chemistry</topic><topic>Inorganic Chemistry</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Measurement Science, Instrumentation</topic></subject><identifier type="issn">0022-5215</identifier><identifier type="issn">Electronic: 1572-8943</identifier><identifier type="matrixNumber">10973</identifier><identifier type="local">IssueArticleCount: 36</identifier><recordInfo><recordOrigin>Wiley Heyden Ltd., Chichester and Akadémiai Kiadó, Budapest, 1992</recordOrigin></recordInfo></relatedItem><identifier type="doi">10.1007/BF01979632</identifier><identifier type="matrixNumber">Art30</identifier><identifier type="local">BF01979632</identifier><accessCondition type="use and reproduction">MetadataGrant: OpenAccess</accessCondition><accessCondition type="use and reproduction">AbstractGrant: OpenAccess</accessCondition><accessCondition type="restriction on access">BodyPDFGrant: Restricted</accessCondition><accessCondition type="restriction on access">BodyHTMLGrant: Restricted</accessCondition><accessCondition type="restriction on access">BibliographyGrant: Restricted</accessCondition><accessCondition type="restriction on access">ESMGrant: Restricted</accessCondition><part><extent unit="pages"><start>2181</start><end>2188</end></extent></part><recordInfo><recordOrigin>Wiley Heyden Ltd., Chichester and Akadémiai Kiadó, Budapest, 1992</recordOrigin><recordIdentifier>10973_1992_Article_BF01979632.pdf</recordIdentifier></recordInfo></mods></record>Pour manipuler ce document sous Unix (Dilib)
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